The fossil assemblage taxonomical composition analysis of upper Coniacianlower Santonian, upper Santonian and lower Campanian deposits is demonstrated. The upper Coniacian and lower Santonian deposits planoconformity has been recorded, the thin upper Santonian deposits presence has been proved and the lower Campanian subface position has been defined. Fractional biostratigraphy subdivision of the Coniacian – lower Campanian interval was carried out. The distinguished strata were traced within Volsk-Khvalynsky district.